REMARK SPARTA+ Protein Chemical Shift Prediction Table REMARK REMARK All chemical shifts are reported in ppm: REMARK REMARK SS_SHIFT is the predicted secondary chemical shift. REMARK SHIFT is the predicted chemical shift. REMARK RC_SHIFT is the random coil chemical shift. REMARK HM_SHIFT is the ring current shift; a correction REMARK of 0.6 times this value is applied. REMARK EF_SHIFT is the adjustment for electric field effect, REMARK applied to proton shifts only. REMARK SIGMA is the estimated prediction error. REMARK REMARK Reference: REMARK Y. Shen and A. Bax: SPARTA+: a modest improvement in empirical NMR REMARK chemical shift prediction by means of an artificial neural network. REMARK J. Biomol. NMR 48, 13-22 (2010). DATA SOURCE 1bz5_1_C DATA FIRST_RESID 1 DATA SEQUENCE RPDFcLEPPY TGPcKARIIR YFYNAKAGLc QTFVYGGcRA KRNNFKSAED DATA SEQUENCE cMRTcG VARS RESID RESNAME ATOMNAME SS_SHIFT SHIFT RC_SHIFT HM_SHIFT EF_SHIFT SIGMA FORMAT %4d %4s %4s %9.3f %9.3f %9.3f %9.3f %9.3f %9.3f 1 R HA 0.000 nan 4.340 nan 0.000 0.208 1 R C 0.000 176.163 176.300 -0.228 0.000 0.893 1 R CA 0.000 55.973 56.100 -0.212 0.000 0.921 1 R CB 0.000 30.126 30.300 -0.290 0.000 0.687 2 P HA 0.155 nan 4.420 nan 0.000 0.269 2 P C -0.333 176.731 177.300 -0.394 0.000 1.215 2 P CA -0.290 62.565 63.100 -0.408 0.000 0.780 2 P CB 0.571 31.791 31.700 -0.801 0.000 0.898 3 D N 0.254 120.538 120.400 -0.194 0.000 2.218 3 D HA -0.114 4.526 4.640 0.000 0.000 0.204 3 D C 1.437 177.726 176.300 -0.018 0.000 0.976 3 D CA 0.965 54.921 54.000 -0.073 0.000 0.853 3 D CB -0.473 40.333 40.800 0.009 0.000 0.939 3 D HN 0.510 nan 8.370 nan 0.000 0.481 4 F N -0.510 119.466 119.950 0.042 0.000 2.451 4 F HA -0.017 4.510 4.527 0.000 0.000 0.299 4 F C 1.779 177.642 175.800 0.104 0.000 1.101 4 F CA -0.117 57.913 58.000 0.049 0.000 1.436 4 F CB -1.273 37.743 39.000 0.026 0.000 1.074 4 F HN -0.078 nan 8.300 nan 0.000 0.553 5 c N 1.283 119.782 118.600 -0.168 0.000 2.449 5 c HA 0.050 4.620 4.570 0.000 0.000 0.283 5 c C 2.524 176.765 174.090 0.251 0.000 1.453 5 c CA 0.442 56.807 56.329 0.060 0.000 1.779 5 c CB -1.642 40.736 42.510 -0.220 0.000 1.779 5 c HN 0.595 nan 8.230 nan 0.000 0.546 6 L N 0.041 121.357 121.223 0.154 0.000 2.567 6 L HA 0.116 4.456 4.340 0.000 0.000 0.225 6 L C 0.781 177.732 176.870 0.136 0.000 1.119 6 L CA 0.438 55.368 54.840 0.150 0.000 0.871 6 L CB -0.386 41.726 42.059 0.087 0.000 1.036 6 L HN 0.278 nan 8.230 nan 0.000 0.459 7 E N 1.170 121.461 120.200 0.153 0.000 2.366 7 E HA 0.252 4.602 4.350 0.000 0.000 0.266 7 E C -2.133 174.507 176.600 0.066 0.000 1.051 7 E CA -1.971 54.486 56.400 0.095 0.000 0.884 7 E CB 0.368 30.120 29.700 0.087 0.000 1.006 7 E HN -0.062 nan 8.360 nan 0.000 0.417 8 P HA 0.153 nan 4.420 nan 0.000 0.274 8 P C -2.349 174.778 177.300 -0.288 0.000 1.231 8 P CA -1.073 61.950 63.100 -0.129 0.000 0.790 8 P CB -0.136 31.505 31.700 -0.098 0.000 0.951 9 P HA 0.005 nan 4.420 nan 0.000 0.268 9 P C -1.398 175.591 177.300 -0.519 0.000 1.205 9 P CA 0.319 62.795 63.100 -1.041 0.000 0.771 9 P CB 0.250 30.781 31.700 -1.949 0.000 0.858 10 Y N 1.570 121.572 120.300 -0.496 0.000 2.338 10 Y HA 0.237 4.787 4.550 0.000 0.000 0.328 10 Y C 1.255 177.250 175.900 0.159 0.000 0.965 10 Y CA -0.131 57.893 58.100 -0.127 0.000 1.208 10 Y CB 1.224 39.649 38.460 -0.059 0.000 1.132 10 Y HN 0.271 nan 8.280 nan 0.000 0.469 11 T N 3.789 118.241 114.554 -0.170 0.000 2.812 11 T HA 0.261 4.611 4.350 0.000 0.000 0.264 11 T C 0.711 175.255 174.700 -0.261 0.000 1.042 11 T CA 1.455 63.553 62.100 -0.003 0.000 1.140 11 T CB -0.736 68.107 68.868 -0.041 0.000 0.870 11 T HN 1.173 nan 8.240 nan 0.000 0.445 12 G N 1.393 109.685 108.800 -0.846 0.000 2.712 12 G HA2 -0.106 3.855 3.960 0.000 0.000 0.683 12 G HA3 -0.106 3.855 3.960 0.000 0.000 0.683 12 G C -2.052 172.669 174.900 -0.300 0.000 1.320 12 G CA -0.309 44.404 45.100 -0.646 0.000 0.847 12 G HN 0.152 nan 8.290 nan 0.000 0.553 13 P HA 0.146 nan 4.420 nan 0.000 0.236 13 P C 1.017 178.258 177.300 -0.099 0.000 1.177 13 P CA 0.674 63.721 63.100 -0.087 0.000 0.773 13 P CB 0.062 31.748 31.700 -0.022 0.000 0.878 14 c N 1.471 119.989 118.600 -0.137 0.000 2.595 14 c HA 0.204 4.774 4.570 0.000 0.000 0.384 14 c C 1.979 175.979 174.090 -0.150 0.000 1.289 14 c CA -0.364 55.878 56.329 -0.145 0.000 2.372 14 c CB 0.491 42.892 42.510 -0.181 0.000 2.593 14 c HN 0.203 nan 8.230 nan 0.000 0.639 15 K N 0.933 121.260 120.400 -0.121 0.000 2.404 15 K HA 0.149 4.469 4.320 0.000 0.000 0.194 15 K C 0.698 177.234 176.600 -0.108 0.000 1.023 15 K CA 0.178 56.404 56.287 -0.102 0.000 1.094 15 K CB -0.382 32.074 32.500 -0.072 0.000 0.841 15 K HN 0.712 nan 8.250 nan 0.000 0.523 16 A N 1.572 124.307 122.820 -0.142 0.000 2.366 16 A HA 0.342 4.662 4.320 0.000 0.000 0.249 16 A C -0.144 177.363 177.584 -0.130 0.000 1.084 16 A CA -0.209 51.750 52.037 -0.130 0.000 0.794 16 A CB 0.252 19.161 19.000 -0.151 0.000 1.034 16 A HN 0.146 nan 8.150 nan 0.000 0.491 17 R N 0.973 121.416 120.500 -0.096 0.000 2.587 17 R HA 0.358 4.698 4.340 0.000 0.000 0.283 17 R C -1.012 175.239 176.300 -0.081 0.000 1.472 17 R CA -0.035 56.014 56.100 -0.083 0.000 1.578 17 R CB 0.413 30.678 30.300 -0.059 0.000 1.130 17 R HN 0.535 nan 8.270 nan 0.000 0.602 18 I N 2.449 122.961 120.570 -0.096 0.000 2.392 18 I HA 0.341 4.511 4.170 0.000 0.000 0.295 18 I C 0.627 176.660 176.117 -0.140 0.000 0.985 18 I CA -1.039 60.212 61.300 -0.081 0.000 1.221 18 I CB 1.400 39.383 38.000 -0.029 0.000 1.366 18 I HN 0.372 nan 8.210 nan 0.000 0.467 19 I N 6.306 126.779 120.570 -0.160 0.000 2.441 19 I HA 0.229 4.399 4.170 0.000 0.000 0.287 19 I C 0.472 176.357 176.117 -0.387 0.000 1.049 19 I CA -0.245 60.888 61.300 -0.278 0.000 1.381 19 I CB 0.427 38.288 38.000 -0.232 0.000 1.409 19 I HN 0.433 nan 8.210 nan 0.000 0.523 20 R N 5.010 125.144 120.500 -0.609 0.000 2.888 20 R HA 0.550 4.890 4.340 0.000 0.000 0.264 20 R C -1.525 174.494 176.300 -0.469 0.000 1.045 20 R CA -1.010 54.760 56.100 -0.550 0.000 0.962 20 R CB 1.969 31.881 30.300 -0.646 0.000 1.210 20 R HN 0.330 nan 8.270 nan 0.000 0.479 21 Y N 0.450 120.923 120.300 0.290 0.000 2.468 21 Y HA 0.550 5.100 4.550 0.000 0.000 0.342 21 Y C 0.067 176.423 175.900 0.759 0.000 1.021 21 Y CA -0.893 57.479 58.100 0.453 0.000 1.079 21 Y CB 1.467 40.086 38.460 0.264 0.000 1.226 21 Y HN 0.482 nan 8.280 nan 0.000 0.460 22 F N -0.059 120.274 119.950 0.638 0.000 2.599 22 F HA 0.590 5.118 4.527 0.000 0.000 0.311 22 F C -1.848 174.188 175.800 0.393 0.000 1.076 22 F CA -1.980 56.319 58.000 0.499 0.000 0.937 22 F CB 0.929 40.028 39.000 0.163 0.000 1.282 22 F HN 0.410 nan 8.300 nan 0.000 0.460 23 Y N 2.764 123.194 120.300 0.216 0.000 2.336 23 Y HA 0.321 4.871 4.550 0.000 0.000 0.335 23 Y C -0.315 175.584 175.900 -0.001 0.000 1.046 23 Y CA -0.530 57.567 58.100 -0.006 0.000 1.198 23 Y CB 0.746 39.252 38.460 0.076 0.000 1.182 23 Y HN 0.863 nan 8.280 nan 0.000 0.502 24 N N 4.803 123.075 118.700 -0.715 0.000 2.558 24 N HA 0.354 5.094 4.740 0.000 0.000 0.233 24 N C 0.662 175.765 175.510 -0.678 0.000 1.038 24 N CA 0.282 53.074 53.050 -0.430 0.000 0.934 24 N CB 0.771 39.042 38.487 -0.361 0.000 1.175 24 N HN 0.890 nan 8.380 nan 0.000 0.512 25 A N 3.485 126.072 122.820 -0.389 0.000 1.940 25 A HA -0.232 4.088 4.320 0.000 0.000 0.219 25 A C 2.375 179.874 177.584 -0.142 0.000 1.176 25 A CA 2.249 54.163 52.037 -0.205 0.000 0.631 25 A CB -0.851 18.199 19.000 0.083 0.000 0.814 25 A HN 0.710 nan 8.150 nan 0.000 0.446 26 K N -0.615 119.723 120.400 -0.102 0.000 2.002 26 K HA 0.179 4.499 4.320 0.000 0.000 0.209 26 K C 2.368 178.916 176.600 -0.086 0.000 1.048 26 K CA 1.996 58.247 56.287 -0.060 0.000 0.930 26 K CB -1.417 31.067 32.500 -0.026 0.000 0.714 26 K HN 1.000 nan 8.250 nan 0.000 0.438 27 A N -0.827 121.913 122.820 -0.134 0.000 2.119 27 A HA 0.397 4.717 4.320 0.000 0.000 0.217 27 A C 2.235 179.727 177.584 -0.153 0.000 1.153 27 A CA 1.407 53.367 52.037 -0.129 0.000 0.692 27 A CB -0.674 18.244 19.000 -0.137 0.000 0.799 27 A HN 1.749 nan 8.150 nan 0.000 0.458 28 G N -1.671 106.984 108.800 -0.241 0.000 2.160 28 G HA2 -0.086 3.874 3.960 0.000 0.000 0.251 28 G HA3 -0.086 3.874 3.960 0.000 0.000 0.251 28 G C -0.093 174.727 174.900 -0.133 0.000 1.008 28 G CA 0.815 45.822 45.100 -0.156 0.000 0.724 28 G HN 1.585 nan 8.290 nan 0.000 0.514 29 L N -4.253 116.778 121.223 -0.320 0.000 2.600 29 L HA 0.847 5.187 4.340 0.000 0.000 0.257 29 L C 0.153 176.862 176.870 -0.269 0.000 1.048 29 L CA -1.788 52.957 54.840 -0.159 0.000 0.869 29 L CB 0.334 42.338 42.059 -0.092 0.000 1.482 29 L HN 0.108 nan 8.230 nan 0.000 0.408 30 c N 0.466 119.003 118.600 -0.106 0.000 2.463 30 c HA 0.759 5.330 4.570 0.000 0.000 0.380 30 c C 0.158 174.160 174.090 -0.146 0.000 1.264 30 c CA -0.087 56.164 56.329 -0.129 0.000 2.161 30 c CB 0.401 42.901 42.510 -0.018 0.000 2.515 30 c HN 0.777 nan 8.230 nan 0.000 0.565 31 Q N 0.326 119.943 119.800 -0.305 0.000 2.528 31 Q HA 0.571 4.912 4.340 0.000 0.000 0.289 31 Q C -0.315 175.762 176.000 0.128 0.000 1.091 31 Q CA -0.556 55.167 55.803 -0.133 0.000 0.797 31 Q CB 2.022 30.603 28.738 -0.263 0.000 1.466 31 Q HN 0.810 nan 8.270 nan 0.000 0.436 32 T N -1.299 113.392 114.554 0.229 0.000 2.918 32 T HA 0.734 5.084 4.350 0.000 0.000 0.283 32 T C -0.485 174.495 174.700 0.466 0.000 1.001 32 T CA -0.487 61.731 62.100 0.197 0.000 1.041 32 T CB 0.452 69.323 68.868 0.006 0.000 1.028 32 T HN 0.514 nan 8.240 nan 0.000 0.511 33 F N -1.084 118.957 119.950 0.152 0.000 2.713 33 F HA 0.668 5.195 4.527 0.001 0.000 0.311 33 F C -1.931 173.895 175.800 0.044 0.000 1.141 33 F CA -1.664 56.404 58.000 0.115 0.000 0.939 33 F CB 0.828 39.873 39.000 0.075 0.000 1.325 33 F HN 0.455 nan 8.300 nan 0.000 0.453 34 V N 3.291 123.209 119.914 0.007 0.000 2.385 34 V HA 0.219 4.339 4.120 0.000 0.000 0.269 34 V C -0.963 175.094 176.094 -0.062 0.000 1.043 34 V CA -0.471 61.761 62.300 -0.113 0.000 0.906 34 V CB 0.571 32.383 31.823 -0.018 0.000 0.995 34 V HN 0.731 nan 8.190 nan 0.000 0.467 35 Y N 3.623 123.696 120.300 -0.378 0.000 2.323 35 Y HA 0.594 5.144 4.550 0.000 0.000 0.331 35 Y C 1.213 177.042 175.900 -0.117 0.000 1.092 35 Y CA -0.814 57.162 58.100 -0.207 0.000 1.150 35 Y CB 1.865 40.145 38.460 -0.300 0.000 1.200 35 Y HN 0.611 nan 8.280 nan 0.000 0.472 36 G N 2.160 110.672 108.800 -0.481 0.000 2.484 36 G HA2 0.245 4.205 3.960 0.000 0.000 0.218 36 G HA3 0.245 4.205 3.960 0.000 0.000 0.218 36 G C 1.019 175.535 174.900 -0.640 0.000 1.130 36 G CA 0.492 45.309 45.100 -0.472 0.000 0.784 36 G HN 1.613 nan 8.290 nan 0.000 0.543 37 G N -1.975 106.044 108.800 -1.301 0.000 2.211 37 G HA2 -0.121 3.839 3.960 0.000 0.000 0.201 37 G HA3 -0.121 3.839 3.960 0.000 0.000 0.201 37 G C 0.318 174.947 174.900 -0.450 0.000 0.997 37 G CA 0.315 44.953 45.100 -0.772 0.000 0.652 37 G HN 1.574 nan 8.290 nan 0.000 0.500 38 c N -1.904 116.445 118.600 -0.418 0.000 3.288 38 c HA 0.833 5.403 4.570 0.000 0.000 0.318 38 c C 0.754 174.942 174.090 0.163 0.000 1.356 38 c CA -0.242 56.077 56.329 -0.017 0.000 1.359 38 c CB 1.522 44.011 42.510 -0.036 0.000 1.688 38 c HN 1.088 nan 8.230 nan 0.000 0.467 39 R N -0.094 120.527 120.500 0.202 0.000 3.333 39 R HA -0.138 4.202 4.340 0.000 0.000 0.256 39 R C 0.422 176.944 176.300 0.370 0.000 1.010 39 R CA 1.055 57.297 56.100 0.237 0.000 0.680 39 R CB -2.060 28.377 30.300 0.228 0.000 1.102 39 R HN 1.476 nan 8.270 nan 0.000 0.440 40 A N 1.224 124.252 122.820 0.346 0.000 2.445 40 A HA 0.331 4.651 4.320 0.000 0.000 0.242 40 A C 0.763 178.387 177.584 0.067 0.000 1.075 40 A CA 0.126 52.302 52.037 0.231 0.000 0.777 40 A CB 0.548 19.500 19.000 -0.079 0.000 1.013 40 A HN 0.178 nan 8.150 nan 0.000 0.493 41 K N 0.474 120.893 120.400 0.032 0.000 2.177 41 K HA 0.314 4.634 4.320 0.000 0.000 0.238 41 K C 1.151 177.632 176.600 -0.198 0.000 1.015 41 K CA -0.733 55.492 56.287 -0.102 0.000 0.922 41 K CB 0.705 33.143 32.500 -0.102 0.000 1.127 41 K HN 0.713 nan 8.250 nan 0.000 0.469 42 R N 0.518 120.840 120.500 -0.297 0.000 2.148 42 R HA -0.091 4.249 4.340 0.000 0.000 0.227 42 R C 0.626 176.628 176.300 -0.497 0.000 1.103 42 R CA 0.760 56.495 56.100 -0.610 0.000 0.983 42 R CB -0.101 29.519 30.300 -1.133 0.000 0.874 42 R HN 0.391 nan 8.270 nan 0.000 0.451 43 N N 1.958 120.625 118.700 -0.055 0.000 3.245 43 N HA -0.034 4.706 4.740 0.000 0.000 0.296 43 N C -1.352 174.226 175.510 0.114 0.000 1.254 43 N CA 0.083 53.267 53.050 0.223 0.000 1.190 43 N CB -0.335 38.380 38.487 0.380 0.000 1.460 43 N HN 0.065 nan 8.380 nan 0.000 0.538 44 N N 2.011 120.580 118.700 -0.218 0.000 2.572 44 N HA 0.207 4.948 4.740 0.000 0.000 0.287 44 N C -1.939 173.358 175.510 -0.355 0.000 1.136 44 N CA -0.256 52.780 53.050 -0.024 0.000 0.900 44 N CB 0.294 38.703 38.487 -0.130 0.000 1.484 44 N HN -0.042 nan 8.380 nan 0.000 0.526 45 F N 1.868 121.967 119.950 0.248 0.000 2.520 45 F HA 0.429 4.956 4.527 0.000 0.000 0.322 45 F C 1.629 177.572 175.800 0.239 0.000 1.103 45 F CA -0.849 57.277 58.000 0.211 0.000 0.926 45 F CB 2.384 41.530 39.000 0.244 0.000 1.154 45 F HN 0.406 nan 8.300 nan 0.000 0.453 46 K N 0.740 121.330 120.400 0.318 0.000 2.167 46 K HA 0.015 4.335 4.320 0.000 0.000 0.203 46 K C 0.466 177.283 176.600 0.362 0.000 1.052 46 K CA 0.699 57.138 56.287 0.253 0.000 0.956 46 K CB 0.224 32.812 32.500 0.147 0.000 0.735 46 K HN 0.474 nan 8.250 nan 0.000 0.451 47 S N -1.000 114.887 115.700 0.312 0.000 2.473 47 S HA 0.494 4.964 4.470 0.000 0.000 0.307 47 S C 0.480 175.025 174.600 -0.093 0.000 1.094 47 S CA -0.458 57.819 58.200 0.129 0.000 1.070 47 S CB 1.744 64.987 63.200 0.072 0.000 1.019 47 S HN 0.280 nan 8.310 nan 0.000 0.480 48 A N 3.560 126.042 122.820 -0.563 0.000 2.015 48 A HA -0.022 4.299 4.320 0.000 0.000 0.219 48 A C 1.905 179.263 177.584 -0.376 0.000 1.163 48 A CA 1.579 53.142 52.037 -0.790 0.000 0.646 48 A CB -0.710 17.674 19.000 -1.026 0.000 0.806 48 A HN 0.964 nan 8.150 nan 0.000 0.448 49 E N 0.054 120.108 120.200 -0.244 0.000 2.051 49 E HA -0.249 4.101 4.350 0.000 0.000 0.192 49 E C 1.137 177.635 176.600 -0.170 0.000 0.991 49 E CA 1.490 57.792 56.400 -0.164 0.000 0.799 49 E CB -0.145 29.497 29.700 -0.098 0.000 0.748 49 E HN 0.535 nan 8.360 nan 0.000 0.449 50 D N 0.191 120.507 120.400 -0.139 0.000 2.144 50 D HA -0.156 4.484 4.640 0.000 0.000 0.199 50 D C 1.980 177.991 176.300 -0.482 0.000 0.984 50 D CA 0.855 54.776 54.000 -0.132 0.000 0.834 50 D CB -0.694 40.165 40.800 0.097 0.000 0.955 50 D HN 0.236 nan 8.370 nan 0.000 0.465 51 c N 0.392 118.569 118.600 -0.705 0.000 2.453 51 c HA -0.071 4.499 4.570 0.000 0.000 0.277 51 c C 2.704 176.444 174.090 -0.584 0.000 1.262 51 c CA 0.546 56.192 56.329 -1.140 0.000 1.718 51 c CB -1.016 41.142 42.510 -0.587 0.000 2.031 51 c HN 0.276 nan 8.230 nan 0.000 0.480 52 M N -0.075 119.322 119.600 -0.338 0.000 2.132 52 M HA -0.117 4.363 4.480 0.000 0.000 0.263 52 M C 2.522 178.691 176.300 -0.219 0.000 1.065 52 M CA 1.881 57.056 55.300 -0.210 0.000 1.122 52 M CB -0.702 31.809 32.600 -0.147 0.000 1.365 52 M HN 0.395 nan 8.290 nan 0.000 0.411 53 R N -0.021 120.354 120.500 -0.208 0.000 2.075 53 R HA -0.101 4.240 4.340 0.000 0.000 0.232 53 R C 1.950 178.152 176.300 -0.163 0.000 1.126 53 R CA 1.832 57.840 56.100 -0.153 0.000 0.963 53 R CB -0.176 30.061 30.300 -0.106 0.000 0.858 53 R HN 0.265 nan 8.270 nan 0.000 0.435 54 T N -0.617 113.817 114.554 -0.199 0.000 2.770 54 T HA -0.097 4.253 4.350 0.000 0.000 0.263 54 T C 1.729 176.290 174.700 -0.232 0.000 1.039 54 T CA 1.328 63.355 62.100 -0.121 0.000 1.142 54 T CB -0.060 68.843 68.868 0.057 0.000 0.868 54 T HN 0.385 nan 8.240 nan 0.000 0.435 55 c N 0.819 119.182 118.600 -0.395 0.000 2.791 55 c HA 0.468 5.038 4.570 0.000 0.000 0.288 55 c C 1.897 175.484 174.090 -0.839 0.000 1.271 55 c CA -1.164 54.761 56.329 -0.674 0.000 1.726 55 c CB -1.001 40.996 42.510 -0.856 0.000 2.145 55 c HN 0.601 nan 8.230 nan 0.000 0.572 56 G N 0.000 108.501 108.800 -0.498 0.000 0.000 56 G HA2 0.000 3.960 3.960 0.000 0.000 0.000 56 G HA3 0.000 3.960 3.960 0.000 0.000 0.000 56 G CA 0.000 44.937 45.100 -0.271 0.000 0.000 56 G HN 0.000 nan 8.290 nan 0.000 0.000