data_25534
#######################
# Entry information #
#######################
save_entry_information
_Entry.Sf_category entry_information
_Entry.Sf_framecode entry_information
_Entry.ID 25534
_Entry.Title
;
RNA structure determination by solid-state NMR spectroscopy
;
_Entry.Type macromolecule
_Entry.Version_type original
_Entry.Submission_date 2015-03-12
_Entry.Accession_date 2015-03-12
_Entry.Last_release_date 2015-05-08
_Entry.Original_release_date 2015-05-08
_Entry.Origination author
_Entry.NMR_STAR_version 3.1.2.6
_Entry.Original_NMR_STAR_version 3.1
_Entry.Experimental_method NMR
_Entry.Experimental_method_subtype SOLID-STATE
_Entry.Details .
_Entry.BMRB_internal_directory_name .
loop_
_Entry_author.Ordinal
_Entry_author.Given_name
_Entry_author.Family_name
_Entry_author.First_initial
_Entry_author.Middle_initials
_Entry_author.Family_title
_Entry_author.ORCID
_Entry_author.Entry_ID
1 Alexander Marchanka . . . . 25534
2 Bernd Simon . . . . 25534
3 Gerhard Althoff-Ospelt . . . . 25534
4 Teresa Carlomagno . . . . 25534
stop_
loop_
_SG_project.SG_project_ID
_SG_project.Project_name
_SG_project.Full_name_of_center
_SG_project.Initial_of_center
_SG_project.Entry_ID
1 'not applicable' 'not applicable' . 25534
stop_
loop_
_Struct_keywords.Keywords
_Struct_keywords.Text
_Struct_keywords.Entry_ID
RNA . 25534
stop_
loop_
_Data_set.Type
_Data_set.Count
_Data_set.Entry_ID
assigned_chemical_shifts 1 25534
stop_
loop_
_Datum.Type
_Datum.Count
_Datum.Entry_ID
'13C chemical shifts' 173 25534
'15N chemical shifts' 49 25534
'31P chemical shifts' 9 25534
stop_
loop_
_Release.Release_number
_Release.Format_type
_Release.Format_version
_Release.Date
_Release.Submission_date
_Release.Type
_Release.Author
_Release.Detail
_Release.Entry_ID
2 . . 2016-08-29 2015-03-12 update BMRB 'update entry citation' 25534
1 . . 2015-05-08 2015-03-12 original author 'original release' 25534
stop_
loop_
_Related_entries.Database_name
_Related_entries.Database_accession_code
_Related_entries.Relationship
_Related_entries.Entry_ID
PDB 2N0R 'BMRB Entry Tracking System' 25534
stop_
save_
###############
# Citations #
###############
save_citations
_Citation.Sf_category citations
_Citation.Sf_framecode citations
_Citation.Entry_ID 25534
_Citation.ID 1
_Citation.Class 'entry citation'
_Citation.CAS_abstract_code .
_Citation.MEDLINE_UI_code .
_Citation.DOI .
_Citation.PubMed_ID 25960310
_Citation.Full_citation .
_Citation.Title
;
RNA structure determination by solid-state NMR spectroscopy
;
_Citation.Status published
_Citation.Type journal
_Citation.Journal_abbrev 'Nat. Commun.'
_Citation.Journal_name_full .
_Citation.Journal_volume 6
_Citation.Journal_issue .
_Citation.Journal_ASTM .
_Citation.Journal_ISSN .
_Citation.Journal_CSD .
_Citation.Book_title .
_Citation.Book_chapter_title .
_Citation.Book_volume .
_Citation.Book_series .
_Citation.Book_publisher .
_Citation.Book_publisher_city .
_Citation.Book_ISBN .
_Citation.Conference_title .
_Citation.Conference_site .
_Citation.Conference_state_province .
_Citation.Conference_country .
_Citation.Conference_start_date .
_Citation.Conference_end_date .
_Citation.Conference_abstract_number .
_Citation.Thesis_institution .
_Citation.Thesis_institution_city .
_Citation.Thesis_institution_country .
_Citation.WWW_URL .
_Citation.Page_first 7024
_Citation.Page_last 7024
_Citation.Year 2015
_Citation.Details .
loop_
_Citation_author.Ordinal
_Citation_author.Given_name
_Citation_author.Family_name
_Citation_author.First_initial
_Citation_author.Middle_initials
_Citation_author.Family_title
_Citation_author.ORCID
_Citation_author.Entry_ID
_Citation_author.Citation_ID
1 Alexander Marchanka . . . . 25534 1
2 Bernd Simon . . . . 25534 1
3 Gerhard Althoff-Ospelt . . . . 25534 1
4 Teresa Carlomagno . . . . 25534 1
stop_
save_
#############################################
# Molecular system (assembly) description #
#############################################
save_assembly
_Assembly.Sf_category assembly
_Assembly.Sf_framecode assembly
_Assembly.Entry_ID 25534
_Assembly.ID 1
_Assembly.Name "26mer Box C/D RNA (5'-R(P*CP*UP*GP*AP*GP*CP*UP*CP*GP*AP*AP*AP*GP*AP*GP*CP*AP*AP*UP*GP*AP*UP*G)-3')"
_Assembly.BMRB_code .
_Assembly.Number_of_components 1
_Assembly.Organic_ligands .
_Assembly.Metal_ions .
_Assembly.Non_standard_bonds .
_Assembly.Ambiguous_conformational_states .
_Assembly.Ambiguous_chem_comp_sites .
_Assembly.Molecules_in_chemical_exchange .
_Assembly.Paramagnetic no
_Assembly.Thiol_state .
_Assembly.Molecular_mass .
_Assembly.Enzyme_commission_number .
_Assembly.Details .
_Assembly.DB_query_date .
_Assembly.DB_query_revised_last_date .
loop_
_Entity_assembly.ID
_Entity_assembly.Entity_assembly_name
_Entity_assembly.Entity_ID
_Entity_assembly.Entity_label
_Entity_assembly.Asym_ID
_Entity_assembly.PDB_chain_ID
_Entity_assembly.Experimental_data_reported
_Entity_assembly.Physical_state
_Entity_assembly.Conformational_isomer
_Entity_assembly.Chemical_exchange_state
_Entity_assembly.Magnetic_equivalence_group_code
_Entity_assembly.Role
_Entity_assembly.Details
_Entity_assembly.Entry_ID
_Entity_assembly.Assembly_ID
1 entity 1 $entity A . yes native no no . . . 25534 1
stop_
save_
####################################
# Biological polymers and ligands #
####################################
save_entity
_Entity.Sf_category entity
_Entity.Sf_framecode entity
_Entity.Entry_ID 25534
_Entity.ID 1
_Entity.BMRB_code .
_Entity.Name '26mer Box C/D RNA'
_Entity.Type polymer
_Entity.Polymer_common_type .
_Entity.Polymer_type polyribonucleotide
_Entity.Polymer_type_details .
_Entity.Polymer_strand_ID A
_Entity.Polymer_seq_one_letter_code_can .
_Entity.Polymer_seq_one_letter_code
;
GCUGAGCUCGAAAGAGCAAU
GAUGUC
;
_Entity.Target_identifier .
_Entity.Polymer_author_defined_seq .
_Entity.Polymer_author_seq_details .
_Entity.Ambiguous_conformational_states no
_Entity.Ambiguous_chem_comp_sites no
_Entity.Nstd_monomer no
_Entity.Nstd_chirality no
_Entity.Nstd_linkage no
_Entity.Nonpolymer_comp_ID .
_Entity.Nonpolymer_comp_label .
_Entity.Number_of_monomers 26
_Entity.Number_of_nonpolymer_components .
_Entity.Paramagnetic no
_Entity.Thiol_state 'not present'
_Entity.Src_method syn
_Entity.Parent_entity_ID .
_Entity.Fragment .
_Entity.Mutation .
_Entity.EC_number .
_Entity.Calc_isoelectric_point .
_Entity.Formula_weight 7450.573
_Entity.Formula_weight_exptl .
_Entity.Formula_weight_exptl_meth .
_Entity.Details .
_Entity.DB_query_date .
_Entity.DB_query_revised_last_date .
loop_
_Entity_comp_index.ID
_Entity_comp_index.Auth_seq_ID
_Entity_comp_index.Comp_ID
_Entity_comp_index.Comp_label
_Entity_comp_index.Entry_ID
_Entity_comp_index.Entity_ID
1 . G . 25534 1
2 . C . 25534 1
3 . U . 25534 1
4 . G . 25534 1
5 . A . 25534 1
6 . G . 25534 1
7 . C . 25534 1
8 . U . 25534 1
9 . C . 25534 1
10 . G . 25534 1
11 . A . 25534 1
12 . A . 25534 1
13 . A . 25534 1
14 . G . 25534 1
15 . A . 25534 1
16 . G . 25534 1
17 . C . 25534 1
18 . A . 25534 1
19 . A . 25534 1
20 . U . 25534 1
21 . G . 25534 1
22 . A . 25534 1
23 . U . 25534 1
24 . G . 25534 1
25 . U . 25534 1
26 . C . 25534 1
stop_
loop_
_Entity_poly_seq.Hetero
_Entity_poly_seq.Mon_ID
_Entity_poly_seq.Num
_Entity_poly_seq.Comp_index_ID
_Entity_poly_seq.Entry_ID
_Entity_poly_seq.Entity_ID
. G 1 1 25534 1
. C 2 2 25534 1
. U 3 3 25534 1
. G 4 4 25534 1
. A 5 5 25534 1
. G 6 6 25534 1
. C 7 7 25534 1
. U 8 8 25534 1
. C 9 9 25534 1
. G 10 10 25534 1
. A 11 11 25534 1
. A 12 12 25534 1
. A 13 13 25534 1
. G 14 14 25534 1
. A 15 15 25534 1
. G 16 16 25534 1
. C 17 17 25534 1
. A 18 18 25534 1
. A 19 19 25534 1
. U 20 20 25534 1
. G 21 21 25534 1
. A 22 22 25534 1
. U 23 23 25534 1
. G 24 24 25534 1
. U 25 25 25534 1
. C 26 26 25534 1
stop_
save_
####################
# Natural source #
####################
save_natural_source
_Entity_natural_src_list.Sf_category natural_source
_Entity_natural_src_list.Sf_framecode natural_source
_Entity_natural_src_list.Entry_ID 25534
_Entity_natural_src_list.ID 1
loop_
_Entity_natural_src.ID
_Entity_natural_src.Entity_ID
_Entity_natural_src.Entity_label
_Entity_natural_src.Entity_chimera_segment_ID
_Entity_natural_src.NCBI_taxonomy_ID
_Entity_natural_src.Type
_Entity_natural_src.Common
_Entity_natural_src.Organism_name_scientific
_Entity_natural_src.Organism_name_common
_Entity_natural_src.Organism_acronym
_Entity_natural_src.ICTVdb_decimal_code
_Entity_natural_src.Superkingdom
_Entity_natural_src.Kingdom
_Entity_natural_src.Genus
_Entity_natural_src.Species
_Entity_natural_src.Strain
_Entity_natural_src.Variant
_Entity_natural_src.Organ
_Entity_natural_src.Tissue
_Entity_natural_src.Tissue_fraction
_Entity_natural_src.Cell_line
_Entity_natural_src.Cell_type
_Entity_natural_src.ATCC_number
_Entity_natural_src.Organelle
_Entity_natural_src.Secretion
_Entity_natural_src.Plasmid
_Entity_natural_src.Gene_mnemonic
_Entity_natural_src.Details
_Entity_natural_src.Entry_ID
_Entity_natural_src.Entity_natural_src_list_ID
1 1 $entity . 562 organism . 'Escherichia coli' 'E. coli' . . Bacteria . Escherichia coli . . . . . . . . . . . . . 25534 1
stop_
save_
#########################
# Experimental source #
#########################
save_experimental_source
_Entity_experimental_src_list.Sf_category experimental_source
_Entity_experimental_src_list.Sf_framecode experimental_source
_Entity_experimental_src_list.Entry_ID 25534
_Entity_experimental_src_list.ID 1
loop_
_Entity_experimental_src.ID
_Entity_experimental_src.Entity_ID
_Entity_experimental_src.Entity_label
_Entity_experimental_src.Entity_chimera_segment_ID
_Entity_experimental_src.Production_method
_Entity_experimental_src.Host_org_scientific_name
_Entity_experimental_src.Host_org_name_common
_Entity_experimental_src.Host_org_details
_Entity_experimental_src.Host_org_NCBI_taxonomy_ID
_Entity_experimental_src.Host_org_genus
_Entity_experimental_src.Host_org_species
_Entity_experimental_src.Host_org_strain
_Entity_experimental_src.Host_org_variant
_Entity_experimental_src.Host_org_ATCC_number
_Entity_experimental_src.Vector_type
_Entity_experimental_src.PDBview_host_org_vector_name
_Entity_experimental_src.PDBview_plasmid_name
_Entity_experimental_src.Vector_name
_Entity_experimental_src.Vector_details
_Entity_experimental_src.Vendor_name
_Entity_experimental_src.Details
_Entity_experimental_src.Entry_ID
_Entity_experimental_src.Entity_experimental_src_list_ID
1 1 $entity . 'enzymatic semisynthesis' . . . . . . . . . . . . . . . . 25534 1
stop_
save_
#####################################
# Sample contents and methodology #
#####################################
########################
# Sample description #
########################
save_sample_1
_Sample.Sf_category sample
_Sample.Sf_framecode sample_1
_Sample.Entry_ID 25534
_Sample.ID 1
_Sample.Type microcrystalline
_Sample.Sub_type .
_Sample.Details .
_Sample.Aggregate_sample_number .
_Sample.Solvent_system H2O
_Sample.Preparation_date .
_Sample.Preparation_expiration_date .
_Sample.Polycrystallization_protocol .
_Sample.Single_crystal_protocol .
_Sample.Crystal_grow_apparatus .
_Sample.Crystal_grow_atmosphere .
_Sample.Crystal_grow_details .
_Sample.Crystal_grow_method .
_Sample.Crystal_grow_method_cit_ID .
_Sample.Crystal_grow_pH .
_Sample.Crystal_grow_pH_range .
_Sample.Crystal_grow_pressure .
_Sample.Crystal_grow_pressure_esd .
_Sample.Crystal_grow_seeding .
_Sample.Crystal_grow_seeding_cit_ID .
_Sample.Crystal_grow_temp .
_Sample.Crystal_grow_temp_details .
_Sample.Crystal_grow_temp_esd .
_Sample.Crystal_grow_time .
_Sample.Oriented_sample_prep_protocol .
_Sample.Lyophilization_cryo_protectant .
_Sample.Storage_protocol .
loop_
_Sample_component.ID
_Sample_component.Mol_common_name
_Sample_component.Isotopic_labeling
_Sample_component.Assembly_ID
_Sample_component.Assembly_label
_Sample_component.Entity_ID
_Sample_component.Entity_label
_Sample_component.Product_ID
_Sample_component.Type
_Sample_component.Concentration_val
_Sample_component.Concentration_val_min
_Sample_component.Concentration_val_max
_Sample_component.Concentration_val_units
_Sample_component.Concentration_val_err
_Sample_component.Vendor
_Sample_component.Vendor_product_name
_Sample_component.Vendor_product_code
_Sample_component.Entry_ID
_Sample_component.Sample_ID
1 entity 'nucleotide-type-selective [U-99% 13C; U-99% 15N]' . . 1 $entity . . 20 . . mg/mL . . . . 25534 1
2 H2O 'natural abundance' . . . . . . 100 . . % . . . . 25534 1
stop_
save_
#######################
# Sample conditions #
#######################
save_sample_conditions_1
_Sample_condition_list.Sf_category sample_conditions
_Sample_condition_list.Sf_framecode sample_conditions_1
_Sample_condition_list.Entry_ID 25534
_Sample_condition_list.ID 1
_Sample_condition_list.Details .
loop_
_Sample_condition_variable.Type
_Sample_condition_variable.Val
_Sample_condition_variable.Val_err
_Sample_condition_variable.Val_units
_Sample_condition_variable.Entry_ID
_Sample_condition_variable.Sample_condition_list_ID
pH 7.5 . pH 25534 1
temperature 260 . K 25534 1
stop_
save_
############################
# Computer software used #
############################
save_CNS
_Software.Sf_category software
_Software.Sf_framecode CNS
_Software.Entry_ID 25534
_Software.ID 1
_Software.Name CNS
_Software.Version 1.2
_Software.Details .
loop_
_Task.Task
_Task.Entry_ID
_Task.Software_ID
'data analysis' 25534 1
stop_
save_
#########################
# Experimental detail #
#########################
##################################
# NMR Spectrometer definitions #
##################################
save_spectrometer_1
_NMR_spectrometer.Sf_category NMR_spectrometer
_NMR_spectrometer.Sf_framecode spectrometer_1
_NMR_spectrometer.Entry_ID 25534
_NMR_spectrometer.ID 1
_NMR_spectrometer.Details .
_NMR_spectrometer.Manufacturer Bruker
_NMR_spectrometer.Model Avance
_NMR_spectrometer.Serial_number .
_NMR_spectrometer.Field_strength 700
save_
save_spectrometer_2
_NMR_spectrometer.Sf_category NMR_spectrometer
_NMR_spectrometer.Sf_framecode spectrometer_2
_NMR_spectrometer.Entry_ID 25534
_NMR_spectrometer.ID 2
_NMR_spectrometer.Details .
_NMR_spectrometer.Manufacturer Bruker
_NMR_spectrometer.Model Avance
_NMR_spectrometer.Serial_number .
_NMR_spectrometer.Field_strength 600
save_
save_NMR_spectrometer_list
_NMR_spectrometer_list.Sf_category NMR_spectrometer_list
_NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list
_NMR_spectrometer_list.Entry_ID 25534
_NMR_spectrometer_list.ID 1
loop_
_NMR_spectrometer_view.ID
_NMR_spectrometer_view.Name
_NMR_spectrometer_view.Manufacturer
_NMR_spectrometer_view.Model
_NMR_spectrometer_view.Serial_number
_NMR_spectrometer_view.Field_strength
_NMR_spectrometer_view.Details
_NMR_spectrometer_view.Citation_ID
_NMR_spectrometer_view.Citation_label
_NMR_spectrometer_view.Entry_ID
_NMR_spectrometer_view.NMR_spectrometer_list_ID
1 spectrometer_1 Bruker Avance . 700 . . . 25534 1
2 spectrometer_2 Bruker Avance . 600 . . . 25534 1
stop_
save_
#############################
# NMR applied experiments #
#############################
save_experiment_list
_Experiment_list.Sf_category experiment_list
_Experiment_list.Sf_framecode experiment_list
_Experiment_list.Entry_ID 25534
_Experiment_list.ID 1
_Experiment_list.Details .
loop_
_Experiment.ID
_Experiment.Name
_Experiment.Raw_data_flag
_Experiment.NMR_spec_expt_ID
_Experiment.NMR_spec_expt_label
_Experiment.MS_expt_ID
_Experiment.MS_expt_label
_Experiment.SAXS_expt_ID
_Experiment.SAXS_expt_label
_Experiment.FRET_expt_ID
_Experiment.FRET_expt_label
_Experiment.EMR_expt_ID
_Experiment.EMR_expt_label
_Experiment.Sample_ID
_Experiment.Sample_label
_Experiment.Sample_state
_Experiment.Sample_volume
_Experiment.Sample_volume_units
_Experiment.Sample_condition_list_ID
_Experiment.Sample_condition_list_label
_Experiment.Sample_spinning_rate
_Experiment.Sample_angle
_Experiment.NMR_tube_type
_Experiment.NMR_spectrometer_ID
_Experiment.NMR_spectrometer_label
_Experiment.NMR_spectrometer_probe_ID
_Experiment.NMR_spectrometer_probe_label
_Experiment.NMR_spectral_processing_ID
_Experiment.NMR_spectral_processing_label
_Experiment.Mass_spectrometer_ID
_Experiment.Mass_spectrometer_label
_Experiment.Xray_instrument_ID
_Experiment.Xray_instrument_label
_Experiment.Fluorescence_instrument_ID
_Experiment.Fluorescence_instrument_label
_Experiment.EMR_instrument_ID
_Experiment.EMR_instrument_label
_Experiment.Chromatographic_system_ID
_Experiment.Chromatographic_system_label
_Experiment.Chromatographic_column_ID
_Experiment.Chromatographic_column_label
_Experiment.Entry_ID
_Experiment.Experiment_list_ID
1 '(13C,15N-TEDOR)-13C,13C PDSD' no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1
2 '13C-31P TEDOR' no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 2 $spectrometer_2 . . . . . . . . . . . . . . . . 25534 1
3 CHHC no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1
4 NHHC no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1
5 CN-TEDOR no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1
stop_
save_
####################
# NMR parameters #
####################
##############################
# Assigned chemical shifts #
##############################
################################
# Chemical shift referencing #
################################
save_chemical_shift_reference_1
_Chem_shift_reference.Sf_category chem_shift_reference
_Chem_shift_reference.Sf_framecode chemical_shift_reference_1
_Chem_shift_reference.Entry_ID 25534
_Chem_shift_reference.ID 1
_Chem_shift_reference.Details .
loop_
_Chem_shift_ref.Atom_type
_Chem_shift_ref.Atom_isotope_number
_Chem_shift_ref.Mol_common_name
_Chem_shift_ref.Atom_group
_Chem_shift_ref.Concentration_val
_Chem_shift_ref.Concentration_units
_Chem_shift_ref.Solvent
_Chem_shift_ref.Rank
_Chem_shift_ref.Chem_shift_units
_Chem_shift_ref.Chem_shift_val
_Chem_shift_ref.Ref_method
_Chem_shift_ref.Ref_type
_Chem_shift_ref.Indirect_shift_ratio
_Chem_shift_ref.External_ref_loc
_Chem_shift_ref.External_ref_sample_geometry
_Chem_shift_ref.External_ref_axis
_Chem_shift_ref.Ref_correction_type
_Chem_shift_ref.Correction_val
_Chem_shift_ref.Entry_ID
_Chem_shift_ref.Chem_shift_reference_ID
C 13 adamantane 'methyl carbons' . . . . ppm 38.48 external direct 1 . . . . . 25534 1
N 15 adamantane 'methyl carbons' . . . . ppm 38.48 na indirect 0.402980 . . . . . 25534 1
P 31 adamantane 'methyl carbons' . . . . ppm 38.48 na indirect 1.609894 . . . . . 25534 1
stop_
save_
###################################
# Assigned chemical shift lists #
###################################
###################################################################
# Chemical Shift Ambiguity Index Value Definitions #
# #
# The values other than 1 are used for those atoms with different #
# chemical shifts that cannot be assigned to stereospecific atoms #
# or to specific residues or chains. #
# #
# Index Value Definition #
# #
# 1 Unique (including isolated methyl protons, #
# geminal atoms, and geminal methyl #
# groups with identical chemical shifts) #
# (e.g. ILE HD11, HD12, HD13 protons) #
# 2 Ambiguity of geminal atoms or geminal methyl #
# proton groups (e.g. ASP HB2 and HB3 #
# protons, LEU CD1 and CD2 carbons, or #
# LEU HD11, HD12, HD13 and HD21, HD22, #
# HD23 methyl protons) #
# 3 Aromatic atoms on opposite sides of #
# symmetrical rings (e.g. TYR HE1 and HE2 #
# protons) #
# 4 Intraresidue ambiguities (e.g. LYS HG and #
# HD protons or TRP HZ2 and HZ3 protons) #
# 5 Interresidue ambiguities (LYS 12 vs. LYS 27) #
# 6 Intermolecular ambiguities (e.g. ASP 31 CA #
# in monomer 1 and ASP 31 CA in monomer 2 #
# of an asymmetrical homodimer, duplex #
# DNA assignments, or other assignments #
# that may apply to atoms in one or more #
# molecule in the molecular assembly) #
# 9 Ambiguous, specific ambiguity not defined #
# #
###################################################################
save_assigned_chem_shift_list_1
_Assigned_chem_shift_list.Sf_category assigned_chemical_shifts
_Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1
_Assigned_chem_shift_list.Entry_ID 25534
_Assigned_chem_shift_list.ID 1
_Assigned_chem_shift_list.Sample_condition_list_ID 1
_Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1
_Assigned_chem_shift_list.Chem_shift_reference_ID 1
_Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1
_Assigned_chem_shift_list.Chem_shift_1H_err .
_Assigned_chem_shift_list.Chem_shift_13C_err .
_Assigned_chem_shift_list.Chem_shift_15N_err .
_Assigned_chem_shift_list.Chem_shift_31P_err .
_Assigned_chem_shift_list.Chem_shift_2H_err .
_Assigned_chem_shift_list.Chem_shift_19F_err .
_Assigned_chem_shift_list.Error_derivation_method .
_Assigned_chem_shift_list.Details .
_Assigned_chem_shift_list.Text_data_format .
_Assigned_chem_shift_list.Text_data .
loop_
_Chem_shift_experiment.Experiment_ID
_Chem_shift_experiment.Experiment_name
_Chem_shift_experiment.Sample_ID
_Chem_shift_experiment.Sample_label
_Chem_shift_experiment.Sample_state
_Chem_shift_experiment.Entry_ID
_Chem_shift_experiment.Assigned_chem_shift_list_ID
1 '(13C,15N-TEDOR)-13C,13C PDSD' . . . 25534 1
2 '13C-31P TEDOR' . . . 25534 1
stop_
loop_
_Atom_chem_shift.ID
_Atom_chem_shift.Assembly_atom_ID
_Atom_chem_shift.Entity_assembly_ID
_Atom_chem_shift.Entity_ID
_Atom_chem_shift.Comp_index_ID
_Atom_chem_shift.Seq_ID
_Atom_chem_shift.Comp_ID
_Atom_chem_shift.Atom_ID
_Atom_chem_shift.Atom_type
_Atom_chem_shift.Atom_isotope_number
_Atom_chem_shift.Val
_Atom_chem_shift.Val_err
_Atom_chem_shift.Assign_fig_of_merit
_Atom_chem_shift.Ambiguity_code
_Atom_chem_shift.Occupancy
_Atom_chem_shift.Resonance_ID
_Atom_chem_shift.Auth_entity_assembly_ID
_Atom_chem_shift.Auth_asym_ID
_Atom_chem_shift.Auth_seq_ID
_Atom_chem_shift.Auth_comp_ID
_Atom_chem_shift.Auth_atom_ID
_Atom_chem_shift.Details
_Atom_chem_shift.Entry_ID
_Atom_chem_shift.Assigned_chem_shift_list_ID
1 . 1 1 2 2 C C2 C 13 158.1 0 . 1 . . . A 2 C C2 . 25534 1
2 . 1 1 3 3 U C1' C 13 93.7 0 . 1 . . . A 3 U C1' . 25534 1
3 . 1 1 3 3 U C2 C 13 154.1 0 . 1 . . . A 3 U C2 . 25534 1
4 . 1 1 3 3 U C2' C 13 75.6 0 . 1 . . . A 3 U C2' . 25534 1
5 . 1 1 3 3 U C3' C 13 71.9 0 . 1 . . . A 3 U C3' . 25534 1
6 . 1 1 3 3 U C4 C 13 165.7 0 . 1 . . . A 3 U C4 . 25534 1
7 . 1 1 3 3 U C4' C 13 82.9 0 . 1 . . . A 3 U C4' . 25534 1
8 . 1 1 3 3 U C5 C 13 104.7 0 . 1 . . . A 3 U C5 . 25534 1
9 . 1 1 3 3 U C5' C 13 64.0 0 . 1 . . . A 3 U C5' . 25534 1
10 . 1 1 3 3 U C6 C 13 139.3 0 . 1 . . . A 3 U C6 . 25534 1
11 . 1 1 3 3 U N1 N 15 145.5 0 . 1 . . . A 3 U N1 . 25534 1
12 . 1 1 3 3 U N3 N 15 157.1 0 . 1 . . . A 3 U N3 . 25534 1
13 . 1 1 4 4 G C1' C 13 90.1 0 . 1 . . . A 4 G C1' . 25534 1
14 . 1 1 4 4 G C2 C 13 156.6 0 . 1 . . . A 4 G C2 . 25534 1
15 . 1 1 4 4 G C2' C 13 76.0 0 . 1 . . . A 4 G C2' . 25534 1
16 . 1 1 4 4 G C3' C 13 79.6 0 . 1 . . . A 4 G C3' . 25534 1
17 . 1 1 4 4 G C4 C 13 155.3 0 . 1 . . . A 4 G C4 . 25534 1
18 . 1 1 4 4 G C4' C 13 88.3 0 . 1 . . . A 4 G C4' . 25534 1
19 . 1 1 4 4 G C5 C 13 116.7 0 . 1 . . . A 4 G C5 . 25534 1
20 . 1 1 4 4 G C5' C 13 67.8 0 . 1 . . . A 4 G C5' . 25534 1
21 . 1 1 4 4 G C6 C 13 160.3 0 . 1 . . . A 4 G C6 . 25534 1
22 . 1 1 4 4 G C8 C 13 139.0 0 . 1 . . . A 4 G C8 . 25534 1
23 . 1 1 4 4 G N1 N 15 145.0 0 . 1 . . . A 4 G N1 . 25534 1
24 . 1 1 4 4 G N2 N 15 81.4 0 . 1 . . . A 4 G N2 . 25534 1
25 . 1 1 4 4 G N9 N 15 167.0 0 . 1 . . . A 4 G N9 . 25534 1
26 . 1 1 4 4 G P P 31 -3.8 0 . 1 . . . A 4 G P . 25534 1
27 . 1 1 5 5 A C1' C 13 88.1 0 . 1 . . . A 5 A C1' . 25534 1
28 . 1 1 5 5 A C2 C 13 156.0 0 . 1 . . . A 5 A C2 . 25534 1
29 . 1 1 5 5 A C2' C 13 78.4 0 . 1 . . . A 5 A C2' . 25534 1
30 . 1 1 5 5 A C3' C 13 80.0 0 . 1 . . . A 5 A C3' . 25534 1
31 . 1 1 5 5 A C4 C 13 150.9 0 . 1 . . . A 5 A C4 . 25534 1
32 . 1 1 5 5 A C4' C 13 83.4 0 . 1 . . . A 5 A C4' . 25534 1
33 . 1 1 5 5 A C5 C 13 118.8 0 . 1 . . . A 5 A C5 . 25534 1
34 . 1 1 5 5 A C5' C 13 70.3 0 . 1 . . . A 5 A C5' . 25534 1
35 . 1 1 5 5 A C6 C 13 156.6 0 . 1 . . . A 5 A C6 . 25534 1
36 . 1 1 5 5 A C8 C 13 139.8 0 . 1 . . . A 5 A C8 . 25534 1
37 . 1 1 5 5 A N6 N 15 81.4 0 . 1 . . . A 5 A N6 . 25534 1
38 . 1 1 5 5 A N9 N 15 166.9 0 . 1 . . . A 5 A N9 . 25534 1
39 . 1 1 5 5 A P P 31 -0.7 0 . 1 . . . A 5 A P . 25534 1
40 . 1 1 6 6 G C1' C 13 92.6 0 . 1 . . . A 6 G C1' . 25534 1
41 . 1 1 6 6 G C2 C 13 158.2 0 . 1 . . . A 6 G C2 . 25534 1
42 . 1 1 6 6 G C2' C 13 75.8 0 . 1 . . . A 6 G C2' . 25534 1
43 . 1 1 6 6 G C3' C 13 77.3 0 . 1 . . . A 6 G C3' . 25534 1
44 . 1 1 6 6 G C4 C 13 152.2 0 . 1 . . . A 6 G C4 . 25534 1
45 . 1 1 6 6 G C4' C 13 83.4 0 . 1 . . . A 6 G C4' . 25534 1
46 . 1 1 6 6 G C5 C 13 119.5 0 . 1 . . . A 6 G C5 . 25534 1
47 . 1 1 6 6 G C5' C 13 70.9 0 . 1 . . . A 6 G C5' . 25534 1
48 . 1 1 6 6 G C6 C 13 157.9 0 . 1 . . . A 6 G C6 . 25534 1
49 . 1 1 6 6 G C8 C 13 139.0 0 . 1 . . . A 6 G C8 . 25534 1
50 . 1 1 6 6 G N1 N 15 148.9 0 . 1 . . . A 6 G N1 . 25534 1
51 . 1 1 6 6 G N2 N 15 75.8 0 . 1 . . . A 6 G N2 . 25534 1
52 . 1 1 6 6 G N9 N 15 171.1 0 . 1 . . . A 6 G N9 . 25534 1
53 . 1 1 6 6 G P P 31 -3.8 0 . 1 . . . A 6 G P . 25534 1
54 . 1 1 7 7 C C1' C 13 93.9 0 . 1 . . . A 7 C C1' . 25534 1
55 . 1 1 7 7 C C2 C 13 159.3 0 . 1 . . . A 7 C C2 . 25534 1
56 . 1 1 7 7 C C2' C 13 75.4 0 . 1 . . . A 7 C C2' . 25534 1
57 . 1 1 7 7 C C3' C 13 72.1 0 . 1 . . . A 7 C C3' . 25534 1
58 . 1 1 7 7 C C4 C 13 168.1 0 . 1 . . . A 7 C C4 . 25534 1
59 . 1 1 7 7 C C4' C 13 82.0 0 . 1 . . . A 7 C C4' . 25534 1
60 . 1 1 7 7 C C5 C 13 97.1 0 . 1 . . . A 7 C C5 . 25534 1
61 . 1 1 7 7 C C5' C 13 64.3 0 . 1 . . . A 7 C C5' . 25534 1
62 . 1 1 7 7 C C6 C 13 142.2 0 . 1 . . . A 7 C C6 . 25534 1
63 . 1 1 7 7 C N1 N 15 152.2 0 . 1 . . . A 7 C N1 . 25534 1
64 . 1 1 7 7 C N3 N 15 196.3 0 . 1 . . . A 7 C N3 . 25534 1
65 . 1 1 7 7 C N4 N 15 100.1 0 . 1 . . . A 7 C N4 . 25534 1
66 . 1 1 8 8 U C1' C 13 93.7 0 . 1 . . . A 8 U C1' . 25534 1
67 . 1 1 8 8 U C2 C 13 152.8 0 . 1 . . . A 8 U C2 . 25534 1
68 . 1 1 8 8 U C2' C 13 75.5 0 . 1 . . . A 8 U C2' . 25534 1
69 . 1 1 8 8 U C3' C 13 72.1 0 . 1 . . . A 8 U C3' . 25534 1
70 . 1 1 8 8 U C4 C 13 169.4 0 . 1 . . . A 8 U C4 . 25534 1
71 . 1 1 8 8 U C4' C 13 82.1 0 . 1 . . . A 8 U C4' . 25534 1
72 . 1 1 8 8 U C5 C 13 103.2 0 . 1 . . . A 8 U C5 . 25534 1
73 . 1 1 8 8 U C5' C 13 64.3 0 . 1 . . . A 8 U C5' . 25534 1
74 . 1 1 8 8 U C6 C 13 142.3 0 . 1 . . . A 8 U C6 . 25534 1
75 . 1 1 8 8 U N1 N 15 145.5 0 . 1 . . . A 8 U N1 . 25534 1
76 . 1 1 8 8 U N3 N 15 163.6 0 . 1 . . . A 8 U N3 . 25534 1
77 . 1 1 9 9 C C1' C 13 93.2 0 . 1 . . . A 9 C C1' . 25534 1
78 . 1 1 9 9 C C2 C 13 158.2 0 . 1 . . . A 9 C C2 . 25534 1
79 . 1 1 9 9 C C2' C 13 75.9 0 . 1 . . . A 9 C C2' . 25534 1
80 . 1 1 9 9 C C3' C 13 71.4 0 . 1 . . . A 9 C C3' . 25534 1
81 . 1 1 9 9 C C4 C 13 168.1 0 . 1 . . . A 9 C C4 . 25534 1
82 . 1 1 9 9 C C4' C 13 81.2 0 . 1 . . . A 9 C C4' . 25534 1
83 . 1 1 9 9 C C5 C 13 98.2 0 . 1 . . . A 9 C C5 . 25534 1
84 . 1 1 9 9 C C5' C 13 64.2 0 . 1 . . . A 9 C C5' . 25534 1
85 . 1 1 9 9 C C6 C 13 140.2 0 . 1 . . . A 9 C C6 . 25534 1
86 . 1 1 9 9 C N1 N 15 151.7 0 . 1 . . . A 9 C N1 . 25534 1
87 . 1 1 9 9 C N3 N 15 197.7 0 . 1 . . . A 9 C N3 . 25534 1
88 . 1 1 9 9 C N4 N 15 99.1 0 . 1 . . . A 9 C N4 . 25534 1
89 . 1 1 10 10 G C1' C 13 94.0 0 . 1 . . . A 10 G C1' . 25534 1
90 . 1 1 10 10 G C2' C 13 75.7 0 . 1 . . . A 10 G C2' . 25534 1
91 . 1 1 10 10 G C3' C 13 71.5 0 . 1 . . . A 10 G C3' . 25534 1
92 . 1 1 10 10 G C4 C 13 155.5 0 . 1 . . . A 10 G C4 . 25534 1
93 . 1 1 10 10 G C4' C 13 81.8 0 . 1 . . . A 10 G C4' . 25534 1
94 . 1 1 10 10 G C5' C 13 64.4 0 . 1 . . . A 10 G C5' . 25534 1
95 . 1 1 10 10 G C6 C 13 161.7 0 . 1 . . . A 10 G C6 . 25534 1
96 . 1 1 10 10 G C8 C 13 136.3 0 . 1 . . . A 10 G C8 . 25534 1
97 . 1 1 10 10 G N1 N 15 146.2 0 . 1 . . . A 10 G N1 . 25534 1
98 . 1 1 10 10 G N2 N 15 75.5 0 . 1 . . . A 10 G N2 . 25534 1
99 . 1 1 10 10 G N9 N 15 171.3 0 . 1 . . . A 10 G N9 . 25534 1
100 . 1 1 14 14 G C1' C 13 92.6 0 . 1 . . . A 14 G C1' . 25534 1
101 . 1 1 14 14 G C2 C 13 157.5 0 . 1 . . . A 14 G C2 . 25534 1
102 . 1 1 14 14 G C2' C 13 74.6 0 . 1 . . . A 14 G C2' . 25534 1
103 . 1 1 14 14 G C4 C 13 151.9 0 . 1 . . . A 14 G C4 . 25534 1
104 . 1 1 14 14 G C5 C 13 119.2 0 . 1 . . . A 14 G C5 . 25534 1
105 . 1 1 14 14 G C5' C 13 69.5 0 . 1 . . . A 14 G C5' . 25534 1
106 . 1 1 14 14 G C8 C 13 137.4 0 . 1 . . . A 14 G C8 . 25534 1
107 . 1 1 14 14 G N1 N 15 148.2 0 . 1 . . . A 14 G N1 . 25534 1
108 . 1 1 14 14 G N2 N 15 75.4 0 . 1 . . . A 14 G N2 . 25534 1
109 . 1 1 14 14 G N9 N 15 170.1 0 . 1 . . . A 14 G N9 . 25534 1
110 . 1 1 15 15 A C1' C 13 92.9 0 . 1 . . . A 15 A C1' . 25534 1
111 . 1 1 15 15 A C2 C 13 153.0 0 . 1 . . . A 15 A C2 . 25534 1
112 . 1 1 15 15 A C2' C 13 75.5 0 . 1 . . . A 15 A C2' . 25534 1
113 . 1 1 15 15 A C3' C 13 72.3 0 . 1 . . . A 15 A C3' . 25534 1
114 . 1 1 15 15 A C4 C 13 148.6 0 . 1 . . . A 15 A C4 . 25534 1
115 . 1 1 15 15 A C4' C 13 81.8 0 . 1 . . . A 15 A C4' . 25534 1
116 . 1 1 15 15 A C5 C 13 120.6 0 . 1 . . . A 15 A C5 . 25534 1
117 . 1 1 15 15 A C5' C 13 65.2 0 . 1 . . . A 15 A C5' . 25534 1
118 . 1 1 15 15 A C6 C 13 157.6 0 . 1 . . . A 15 A C6 . 25534 1
119 . 1 1 15 15 A C8 C 13 139.5 0 . 1 . . . A 15 A C8 . 25534 1
120 . 1 1 15 15 A N1 N 15 222.1 0 . 1 . . . A 15 A N1 . 25534 1
121 . 1 1 15 15 A N9 N 15 171.5 0 . 1 . . . A 15 A N9 . 25534 1
122 . 1 1 16 16 G C1' C 13 92.5 0 . 1 . . . A 16 G C1' . 25534 1
123 . 1 1 16 16 G C2 C 13 157.0 0 . 1 . . . A 16 G C2 . 25534 1
124 . 1 1 16 16 G C2' C 13 75.8 0 . 1 . . . A 16 G C2' . 25534 1
125 . 1 1 16 16 G C3' C 13 72.0 0 . 1 . . . A 16 G C3' . 25534 1
126 . 1 1 16 16 G C4 C 13 151.6 0 . 1 . . . A 16 G C4 . 25534 1
127 . 1 1 16 16 G C4' C 13 81.7 0 . 1 . . . A 16 G C4' . 25534 1
128 . 1 1 16 16 G C5 C 13 119.0 0 . 1 . . . A 16 G C5 . 25534 1
129 . 1 1 16 16 G C5' C 13 64.3 0 . 1 . . . A 16 G C5' . 25534 1
130 . 1 1 16 16 G C6 C 13 160.9 0 . 1 . . . A 16 G C6 . 25534 1
131 . 1 1 16 16 G C8 C 13 135.6 0 . 1 . . . A 16 G C8 . 25534 1
132 . 1 1 16 16 G N1 N 15 148.0 0 . 1 . . . A 16 G N1 . 25534 1
133 . 1 1 16 16 G N2 N 15 74.6 0 . 1 . . . A 16 G N2 . 25534 1
134 . 1 1 16 16 G N9 N 15 170.9 0 . 1 . . . A 16 G N9 . 25534 1
135 . 1 1 17 17 C C1' C 13 93.6 0 . 1 . . . A 17 C C1' . 25534 1
136 . 1 1 17 17 C C2 C 13 158.5 0 . 1 . . . A 17 C C2 . 25534 1
137 . 1 1 17 17 C C2' C 13 75.7 0 . 1 . . . A 17 C C2' . 25534 1
138 . 1 1 17 17 C C3' C 13 71.7 0 . 1 . . . A 17 C C3' . 25534 1
139 . 1 1 17 17 C C4 C 13 167.6 0 . 1 . . . A 17 C C4 . 25534 1
140 . 1 1 17 17 C C4' C 13 81.6 0 . 1 . . . A 17 C C4' . 25534 1
141 . 1 1 17 17 C C5 C 13 97.9 0 . 1 . . . A 17 C C5 . 25534 1
142 . 1 1 17 17 C C5' C 13 64.1 0 . 1 . . . A 17 C C5' . 25534 1
143 . 1 1 17 17 C C6 C 13 139.0 0 . 1 . . . A 17 C C6 . 25534 1
144 . 1 1 17 17 C N1 N 15 150.5 0 . 1 . . . A 17 C N1 . 25534 1
145 . 1 1 17 17 C N3 N 15 195.9 0 . 1 . . . A 17 C N3 . 25534 1
146 . 1 1 17 17 C N4 N 15 99.0 0 . 1 . . . A 17 C N4 . 25534 1
147 . 1 1 18 18 A C1' C 13 94.1 0 . 1 . . . A 18 A C1' . 25534 1
148 . 1 1 18 18 A C2 C 13 156.0 0 . 1 . . . A 18 A C2 . 25534 1
149 . 1 1 18 18 A C2' C 13 76.6 0 . 1 . . . A 18 A C2' . 25534 1
150 . 1 1 18 18 A C3' C 13 72.5 0 . 1 . . . A 18 A C3' . 25534 1
151 . 1 1 18 18 A C4 C 13 150.6 0 . 1 . . . A 18 A C4 . 25534 1
152 . 1 1 18 18 A C4' C 13 81.6 0 . 1 . . . A 18 A C4' . 25534 1
153 . 1 1 18 18 A C5 C 13 121.6 0 . 1 . . . A 18 A C5 . 25534 1
154 . 1 1 18 18 A C5' C 13 64.6 0 . 1 . . . A 18 A C5' . 25534 1
155 . 1 1 18 18 A C6 C 13 157.7 0 . 1 . . . A 18 A C6 . 25534 1
156 . 1 1 18 18 A C8 C 13 138.6 0 . 1 . . . A 18 A C8 . 25534 1
157 . 1 1 18 18 A N6 N 15 80.7 0 . 1 . . . A 18 A N6 . 25534 1
158 . 1 1 18 18 A N7 N 15 230.9 0 . 1 . . . A 18 A N7 . 25534 1
159 . 1 1 18 18 A N9 N 15 173.2 0 . 1 . . . A 18 A N9 . 25534 1
160 . 1 1 18 18 A P P 31 -4.2 0 . 1 . . . A 18 A P . 25534 1
161 . 1 1 19 19 A C1' C 13 89.7 0 . 1 . . . A 19 A C1' . 25534 1
162 . 1 1 19 19 A C2 C 13 154.5 0 . 1 . . . A 19 A C2 . 25534 1
163 . 1 1 19 19 A C2' C 13 72.2 0 . 1 . . . A 19 A C2' . 25534 1
164 . 1 1 19 19 A C3' C 13 78.5 0 . 1 . . . A 19 A C3' . 25534 1
165 . 1 1 19 19 A C4 C 13 150.5 0 . 1 . . . A 19 A C4 . 25534 1
166 . 1 1 19 19 A C4' C 13 85.1 0 . 1 . . . A 19 A C4' . 25534 1
167 . 1 1 19 19 A C5 C 13 121.8 0 . 1 . . . A 19 A C5 . 25534 1
168 . 1 1 19 19 A C5' C 13 67.4 0 . 1 . . . A 19 A C5' . 25534 1
169 . 1 1 19 19 A C6 C 13 156.4 0 . 1 . . . A 19 A C6 . 25534 1
170 . 1 1 19 19 A C8 C 13 145.8 0 . 1 . . . A 19 A C8 . 25534 1
171 . 1 1 19 19 A N6 N 15 76.3 0 . 1 . . . A 19 A N6 . 25534 1
172 . 1 1 19 19 A N7 N 15 228.2 0 . 1 . . . A 19 A N7 . 25534 1
173 . 1 1 19 19 A N9 N 15 164.7 0 . 1 . . . A 19 A N9 . 25534 1
174 . 1 1 19 19 A P P 31 -1.8 0 . 1 . . . A 19 A P . 25534 1
175 . 1 1 20 20 U C1' C 13 89.4 0 . 1 . . . A 20 U C1' . 25534 1
176 . 1 1 20 20 U C2 C 13 154.2 0 . 1 . . . A 20 U C2 . 25534 1
177 . 1 1 20 20 U C2' C 13 75.4 0 . 1 . . . A 20 U C2' . 25534 1
178 . 1 1 20 20 U C3' C 13 80.5 0 . 1 . . . A 20 U C3' . 25534 1
179 . 1 1 20 20 U C4 C 13 167.9 0 . 1 . . . A 20 U C4 . 25534 1
180 . 1 1 20 20 U C4' C 13 84.2 0 . 1 . . . A 20 U C4' . 25534 1
181 . 1 1 20 20 U C5 C 13 105.7 0 . 1 . . . A 20 U C5 . 25534 1
182 . 1 1 20 20 U C5' C 13 69.5 0 . 1 . . . A 20 U C5' . 25534 1
183 . 1 1 20 20 U C6 C 13 146.8 0 . 1 . . . A 20 U C6 . 25534 1
184 . 1 1 20 20 U N1 N 15 147.4 0 . 1 . . . A 20 U N1 . 25534 1
185 . 1 1 20 20 U N3 N 15 158.5 0 . 1 . . . A 20 U N3 . 25534 1
186 . 1 1 20 20 U P P 31 -5.3 0 . 1 . . . A 20 U P . 25534 1
187 . 1 1 21 21 G C1' C 13 87.5 0 . 1 . . . A 21 G C1' . 25534 1
188 . 1 1 21 21 G C2' C 13 77.5 0 . 1 . . . A 21 G C2' . 25534 1
189 . 1 1 21 21 G C3' C 13 80.0 0 . 1 . . . A 21 G C3' . 25534 1
190 . 1 1 21 21 G C4 C 13 155.7 0 . 1 . . . A 21 G C4 . 25534 1
191 . 1 1 21 21 G C4' C 13 87.5 0 . 1 . . . A 21 G C4' . 25534 1
192 . 1 1 21 21 G C5 C 13 117.6 0 . 1 . . . A 21 G C5 . 25534 1
193 . 1 1 21 21 G C5' C 13 68.3 0 . 1 . . . A 21 G C5' . 25534 1
194 . 1 1 21 21 G C6 C 13 160.3 0 . 1 . . . A 21 G C6 . 25534 1
195 . 1 1 21 21 G C8 C 13 139.1 0 . 1 . . . A 21 G C8 . 25534 1
196 . 1 1 21 21 G N1 N 15 145.6 0 . 1 . . . A 21 G N1 . 25534 1
197 . 1 1 21 21 G N2 N 15 81.0 0 . 1 . . . A 21 G N2 . 25534 1
198 . 1 1 21 21 G N9 N 15 168.8 0 . 1 . . . A 21 G N9 . 25534 1
199 . 1 1 21 21 G P P 31 -6.0 0 . 1 . . . A 21 G P . 25534 1
200 . 1 1 22 22 A C1' C 13 92.4 0 . 1 . . . A 22 A C1' . 25534 1
201 . 1 1 22 22 A C2 C 13 156.0 0 . 1 . . . A 22 A C2 . 25534 1
202 . 1 1 22 22 A C2' C 13 75.7 0 . 1 . . . A 22 A C2' . 25534 1
203 . 1 1 22 22 A C3' C 13 72.4 0 . 1 . . . A 22 A C3' . 25534 1
204 . 1 1 22 22 A C4 C 13 147.5 0 . 1 . . . A 22 A C4 . 25534 1
205 . 1 1 22 22 A C4' C 13 82.9 0 . 1 . . . A 22 A C4' . 25534 1
206 . 1 1 22 22 A C5 C 13 120.8 0 . 1 . . . A 22 A C5 . 25534 1
207 . 1 1 22 22 A C5' C 13 65.8 0 . 1 . . . A 22 A C5' . 25534 1
208 . 1 1 22 22 A C6 C 13 157.1 0 . 1 . . . A 22 A C6 . 25534 1
209 . 1 1 22 22 A C8 C 13 140.0 0 . 1 . . . A 22 A C8 . 25534 1
210 . 1 1 22 22 A N6 N 15 81.2 0 . 1 . . . A 22 A N6 . 25534 1
211 . 1 1 22 22 A N9 N 15 170.2 0 . 1 . . . A 22 A N9 . 25534 1
212 . 1 1 22 22 A P P 31 -0.1 0 . 1 . . . A 22 A P . 25534 1
213 . 1 1 23 23 U C1' C 13 93.0 0 . 1 . . . A 23 U C1' . 25534 1
214 . 1 1 23 23 U C2 C 13 151.0 0 . 1 . . . A 23 U C2 . 25534 1
215 . 1 1 23 23 U C2' C 13 74.6 0 . 1 . . . A 23 U C2' . 25534 1
216 . 1 1 23 23 U C3' C 13 72.1 0 . 1 . . . A 23 U C3' . 25534 1
217 . 1 1 23 23 U C4 C 13 167.6 0 . 1 . . . A 23 U C4 . 25534 1
218 . 1 1 23 23 U C4' C 13 82.3 0 . 1 . . . A 23 U C4' . 25534 1
219 . 1 1 23 23 U C5 C 13 103.8 0 . 1 . . . A 23 U C5 . 25534 1
220 . 1 1 23 23 U C5' C 13 63.1 0 . 1 . . . A 23 U C5' . 25534 1
221 . 1 1 23 23 U C6 C 13 140.0 0 . 1 . . . A 23 U C6 . 25534 1
222 . 1 1 23 23 U N1 N 15 144.7 0 . 1 . . . A 23 U N1 . 25534 1
223 . 1 1 23 23 U N3 N 15 155.7 0 . 1 . . . A 23 U N3 . 25534 1
224 . 1 1 23 23 U P P 31 -4.2 0 . 1 . . . A 23 U P . 25534 1
225 . 1 1 24 24 G C1' C 13 92.6 0 . 1 . . . A 24 G C1' . 25534 1
226 . 1 1 24 24 G C2 C 13 157.4 0 . 1 . . . A 24 G C2 . 25534 1
227 . 1 1 24 24 G C4 C 13 152.9 0 . 1 . . . A 24 G C4 . 25534 1
228 . 1 1 24 24 G C5 C 13 118.1 0 . 1 . . . A 24 G C5 . 25534 1
229 . 1 1 24 24 G C8 C 13 136.2 0 . 1 . . . A 24 G C8 . 25534 1
230 . 1 1 24 24 G N2 N 15 76.5 0 . 1 . . . A 24 G N2 . 25534 1
231 . 1 1 24 24 G N9 N 15 172.4 0 . 1 . . . A 24 G N9 . 25534 1
stop_
save_