BMRB Entry 10022
Click here to enlarge.
PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR10022
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
NMR-STAR v2.1 text file (deprecated)
XML gzip file.
RDF gzip file.
All files associated with the entry
Title: 3D Structure of amyloid protofibrils of beta2-microglobulin fragment probed by solid-state NMR PubMed: 17108084
Deposition date: 2006-06-27 Original release date: 2006-10-26
Authors: Iwata, Kentaro; Fujiwara, Toshimichi; Matsuki, Yoh; Akutsu, Hideo; Takahashi, Satoshi; Naiki, Hironobu; Goto, Yuji
Citation: Iwata, Kentaro; Fujiwara, Toshimichi; Matsuki, Yoh; Akutsu, Hideo; Takahashi, Satoshi; Naiki, Hironobu; Goto, Yuji. "3D Structure of amyloid protofibrils of beta2-microglobulin fragment probed by solid-state NMR" Proc. Natl. Acad. Sci. U.S.A. 103, 18119-18124 (2006).
Assembly members:
amyloid protofibrils of beta2-microglobulin fragment, polymer, 22 residues, Formula weight is not available
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
amyloid protofibrils of beta2-microglobulin fragment: SNFLNCYVSGFHPSDIEVDL
LK
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 113 |
| 15N chemical shifts | 26 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | K3 peptide of beta2-microglobulin | 1 |
Entities:
Entity 1, K3 peptide of beta2-microglobulin 22 residues - Formula weight is not available
| 1 | SER | ASN | PHE | LEU | ASN | CYS | TYR | VAL | SER | GLY | ||||
| 2 | PHE | HIS | PRO | SER | ASP | ILE | GLU | VAL | ASP | LEU | ||||
| 3 | LEU | LYS |
Samples:
sample_1: amyloid protofibrils of beta2-microglobulin fragment 10 ± 2 mg
condition_1: temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D-3D-13C-13C-RFDR | sample_1 | not available | condition_1 |
| 2D-3D-13C-13C-DARR | sample_1 | not available | condition_1 |
| 2D-13C-13C-SPCz5 | sample_1 | not available | condition_1 |
| 2D-13C-13C-INADEQUATE | sample_1 | not available | condition_1 |
| 2D-3D-15N-13C-RFDR | sample_1 | not available | condition_1 |
| 3D-15N-13C-SPECIFIC_CP | sample_1 | not available | condition_1 |
| 2D-13C-HH-13C-SPIN_DIFF | not available | not available | not available |
Software:
No software information available
NMR spectrometers:
- Varian Infinity-500 500 MHz
- Varian Infinity-600 600 MHz
- Varian Infinity-700 700 MHz
Related Database Links:
| BMRB | 15480 16587 17165 17166 19099 19113 19116 19118 19119 19120 19121 19122 19123 3078 3079 |
| PDB | |
| DBJ | BAA35182 BAE01010 BAE87778 BAG38125 BAG64583 |
| EMBL | CAA23830 CAG33347 CAH92078 |
| GB | AAA87972 AAA88008 AAA88837 AAB25312 AAB31321 |
| REF | NP_001009066 NP_001040602 NP_001127503 NP_001167006 NP_001271618 |
| SP | O77517 O77518 O77519 O77520 O77521 |