BMRB Entry 7397
Click here to enlarge.
PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR7397
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
NMR-STAR v2.1 text file (deprecated)
XML gzip file.
RDF gzip file.
All files associated with the entry
Title: Purification and structural characterization of a D-amino acid containing conopeptide, marmophine, from Conus marmoreus PubMed: 18355315
Deposition date: 2007-06-29 Original release date: 2008-06-17
Authors: Huang, F.; Du, W.; Han, Y.; Wang, C.
Citation: Han, Y.; Huang, F.; Jiang, H.; Liu, L.; Wang, Q.; Wang, Y.; Shao, X.; Chi, C.; Du, W.; Wang, C.. "Purification and structural characterization of a D-amino acid-containing conopeptide, conomarphin, from Conus marmoreus" FEBS J. 275, 1976-1987 (2008).
Assembly members:
M-conotoxin_mr12, polymer, 15 residues, Formula weight is not available
Natural source: Common Name: Shigella flexneri Taxonomy ID: 623 Superkingdom: Bacteria Kingdom: not available Genus/species: Shigella flexneri
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
M-conotoxin_mr12: DWEYHAHPKXNSXWT
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 82 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | M-conotoxin_mr12 | 1 |
Entities:
Entity 1, M-conotoxin_mr12 15 residues - Formula weight is not available
| 1 | ASP | TRP | GLU | TYR | HIS | ALA | HIS | PRO | LYS | HYP | ||||
| 2 | ASN | SER | DPN | TRP | THR |
Samples:
sample_1: M-conotoxin_mr12 2.0 mM; H2O 90%; D2O 10%
sample_2: M-conotoxin_mr12 2.0 mM; D2O 99.99%
sample_conditions_1: pH: 3.0; pressure: 1 atm; temperature: 300 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | isotropic | sample_conditions_1 |
| 2D TOCSY | not available | isotropic | sample_conditions_1 |
| DQF-COSY | not available | isotropic | sample_conditions_1 |
| 2D NOESY | not available | isotropic | sample_conditions_1 |
| 2D TOCSY | not available | isotropic | sample_conditions_1 |
| DQF-COSY | not available | isotropic | sample_conditions_1 |
Software:
xwinnmr v3.5, Bruker Inc. - collection
TOPSPIN v1.3B, Bruker Inc. - processing
SPARKY v3.110, T. D. Goddard and D. G. Kneller - structure solution
CYANA v2.1, L. A. Systems, Inc. - structure solution
AMBER v9.0 - refinement
NMR spectrometers:
- Bruker AVANCE 600 MHz